deformation is 0.7 um [99Gee]. The EBSD information depth for this material is estimated to be
about 0.04 um at 20 kV [93Joy], [98Ren]. nz
Pattern Quality as a Measure for Preparation Quality
A reliable automatic EBSD scan is only possible if the EBSPs are of good quality (contrast) so that
they can be recognized by the computer. Lines in the pattern are transformed by Hough transform in
points in the Hough space for easier and faster location (Fig. 3) [92Kri]. The average height of the
detected peaks in the Hough transform can be used as a quality parameter [94 War], [98TSL].
(X4,Yı)
P {ad
Bays)
) PQl = 205
Fig. 3: Line detection for indexing of EBSP
It should be noticed that the so defined pattern quality index (PQI) is also dependent on other
factors like crystal system, orientation, etc. Nevertheless it is a very good measure, even not
absolute, for the strain in the diffraction volume of material (Fig. 4). For automatic scans a PQI
above 80 is desirable. But depending on the crystal symmetry and orientation pattern with much
lower PQI can be indexed correctly as well.
MM
mate
best
Wh
ny
may
Fig. 4: EBSP of different quality index due to different preparation (Iron, 20 kV) a
Preparation for EBSD
Different materials were prepared so that EBSPs of good quality were obtained. The test materials | N
differ in hardness, which strongly influences the preparation behaviour, and also in their EBSD a
information depth. In Fig 5 they are plotted by hardness versus the escape depth of the .
356