174 Prakt. Met. Sonderband 46 (2014)
5. SUMMARY VERB!
The strength distribution of different glass-ceramic composite systems was determined VON §
using a biaxial strength testing method (the Ball-on-three-balls test). Bulk substrates with ANWE
different microstructure were compared with multilayer architectures combining two
different materials. An increase in strength was measured in the multilayer composites W. Harre
related to the compressive stresses in the surface layers, generated during sintering due eo
to the different thermal expansion coefficients of the combined microstructures. The Institut fi
residual stress in the surface layers measured with Raman spectroscopy was in FCT Inc
agreement with the increase in strength with respect to the bulk samples.
ACKNOWLEDGEMENTS
ABSTR
Financial support by the Austrian Federal Government (in particular from the Bundesministerium fiir Verkehr,
Innovation und Technologie and the Bundesministerium fur Wirtschaft und Arbeit) and the Styrian Provincial Aufgrund
Government, represented by Osterreichische Forschungsforderungsgesellschaft mbH and by Steirische SisNg in
Wirtschaftsforderungsgeselischaft mbH, within the research activities of the K2 Competence Centre on CL
“Integrated Research in Materials, Processing and Product Engineering’, operated by the Materials Center Bei einig‘
Leoben Forschung GmbH in the framework of the Austrian COMET Competence Centre Programme, is Versagen
gratefully acknowledged. startet vo
oft durcl
REFERENCES gefährlich
[1] Ewsuk, K. G.: "Ceramic-filled-glass composite sintering", Ceramic Transactions, 15, gelungen
1990, p. 279. J
[2] Bermejo, R., Torres, Y., Sanchez-Herencia, A. J., Baudin, C., Anglada, M., Llanes, L.: dass die
"Residual stresses, strength and toughness of laminates with different layer thickness von Baut
ratios", Acta Mater., 54, 2006, p. 4745. der Geon
[3] O&l, H. J., Fréchette, V. D.: "Stress distribution in multiphase systems: I, composites ein Weg
with planar interfaces", J. Am. Ceram. Soc., 50, 1967, p. 542. und Stan
[4] Sestakova, L., Bermejo, R., Chlup, Z., Danzer, R.: "Strategies for fracture toughness,
strength and reliability optimisation of ceramic-ceramic laminates”, Int. J. Mat. Res,
102, 2011, p. 613. 1. EINL!
[5] Bermejo, R., Supancic, P., Kraleva, |., Morrell, R., Danzer, R.: "Strength reliability of 3D ’
low temperature co-fired multilayer ceramics under biaxial loading", J. Eur. Ceram. Auf
Soc., 31, 2011, p. 745. yy grund
[6] Borger, A., Supancic, P., Danzer, R.: "The ball on three balls test for strength testing of empera
brittle discs: stress distribution in the disc", J. Eur. Ceram. Soc., 22, 2002, p. 1425. o durch
[7] Danzer, R., Supancic, P., Harrer, W.: "Biaxial Tensile Strength Test for Brittle open u
Rectangular Plates", J. Ceram. Soc. Jpn., 114, 2006, p. 1054. ray
[8] Bermejo, R., Supancic, P., Krautgasser, C., Morrell, R., Danzer, R.: "Subcritical Crack 0 J. Eine
Growth in Low Temperature Co-fired Ceramics under Biaxial Loading", Eng. Fract. I iol
Mech., 100, 2013, p. 108. I vielen
[9] Freiman, S. W., Wiederhorn, S. M., Mecholsky, J. J. "Environmentally Enhanced "aa
Fracture of Glass: A Historical Perspective", J. Am. Ceram. Soc., 92, 2009, p. 1371. von A
[10] Ma, Q., Clarke, D. R.: "Piezospectroscopic Determination of Residual Stresses in eine N
Polycrystahe Alumina”, J. Am. Ceram. Soc., 77, 1994, p. 298. wirkor A
[11] Pascual, J., Lube, T., Danzer, R.: "Fracture statistics of ceramic laminates das iy
strengthened by compressive residual stresses". J. Eur. Ceram. Soc., 28, 2008, p. Siliviurm
1551. :
[12] EN 843-5, Advanced Technical Ceramics - Monolithic Ceramics - Mechanical Tests at Lom) st
Room Temperature - Part 5: Statistical Analysis, pp. 40. In EN 843-5. 1997. SEO