Full text: Fortschritte in der Metallographie

Prakt. Met. Sonderband 52 (2018) 127 
MICROSTRUCTURAL CHARACTERISATION OF A HIGH 
ENTROPY ALLOY 
M. Speicher”, R. Scheck, D. Willer", J. Wagner? 
1) Materials Testing Institute (MPA), University of Stuttgart, Stuttgart, Germany 
2) previously Institute of Materials Science, University of Stuttgart, Stuttgart, Germany 
_ ABSTRACT 
Yoox ver | In this work the microstructure as well as the precipitation structure of a high entropy alloy 
Al-Cu-Ni-Ti-V with an equiatomic composition (AI20Fe20Ni20Ti20V20 in at.%) was 
investigated on several length scales. Different material states before and after heat 
treatment were characterized by optical and scanning electron microscopy and 3D atom 
probe tomography. In addition, the phases were identified by X-ray diffraction and the 
mechanical properties were determined in the compression tests. 
1. INTRODUCTION 
rlyische High entropy alloys (HEA) is a quite novel group of metallic materials. These alloys consist 
Ava of near-equiatomic concentrations of several metallic elements. They fundamentally differ 
ss from conventional alloys, which commonly consist of a primary element with additions of 
felfol alloying elements in order to achieve desired properties. This new concept of alloy design 
with no base element opens up a huge multi-component space with significant 
technological potential and poses challenging scientific questions. Due to the intrinsic and 
specially emphasized microstructural properties of high entropy alloys, like high lattice 
strains or locally strongly changing chemical potentials, one could use these properties to 
echanisch ind develop a hydrogen resistant HEA. Hydrogen embrittlement (HE) is observed in a large 
Co variety of metallic materials (i.e. Al, Ni, Fe and their alloys) and applications [1]. Since HE 
Weg corresponds to decreasing fracture toughness, it is an important industrial and technical 
er. De problem. Additionally, with the depletion of fossil fuels, hydrogen is believed to be a 
It, ist fiir Mg- possible energy source in future. Thus, for the efficient and effective use of hydrogen, safe 
> mechanische hydrogen storage and transportation, e.g. to and from hydrogen fuel cells or large-scale 
sien sodas Production facilities will become necessary. To develop tailored materials for this purpose, 
n Phasen und however, is still challenging, since the interactions of hydrogen with metals at different 
time- and length scales are still not fully understood. Currently, there are only a few studies 
en geal about the usage of HEA in hydrogen rich environments, most of them dealing with the 
aratonsgerale ability of HEA to store hydrogen for future energy purposes [2-4]. 
uf kommen mit In this study the first results on the microstructure and mechanical properties of a Al-Cu-Ni- 
Präparationen Ti-V alloy with an equiatomic composition (Al20Fe20Ni20Ti20V20 in at.%) are presented. 
rerich. Beide The aim for the developing of this alloy is to design material resistant again the hydrogen 
embrittlement. 
Iremen, Leibniz 
ingen, Struers
	        
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