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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 177. Pimelinsäure.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

OU 
     
— 138 — 
175. Brenzweinsáure. 
C,H,0, = CH, - CH(COOH) - CH, - COOH. 
Trikline Prismen!, P. 112,5?? (aus Wasser). Beim Erhitzen auf 200? ent- 
steht das Anhydrid, F. 31,5—32^?, Ky. 247,9? (korr.)?. 
Nachweis. Diamid*. F. 225°, 
Phenacylester?. F. 101,5° (aus verd. Alkohol). 
Chininsalz9. F. 174—175? (aus Alkohol). 
Bestimmung durch Titration in üblicher Weise. 
  
C,H,0, M.G.132 
C 45,4 96 
H 6,1% 
  
  
  
  
a 176. Adipinsäure. 
C,H440, — HOOC - CH, - CH, - CH, - CH, - COOH. 
Monoklin-prismatische Krystalle (aus Essigester" oder besser Salpetersáure 
B 1,428), F. 153—154? (korr.)?, Kp.,99 265? 9. 
E Nachweis. Silbersalz8. Blättchen (aus Wasser). 
E Diamid!. Krystallines Pulver, F. 220? (aus Wasser). 
Dhydrazid??. Blätter, F. 171? (aus Wasser oder verd. Alkohol). 
Phenacylester'®. F. 87,6° (aus Aceton). 
p-Phenylphenacylester!*. F. 148° (aus Aceton). 
p-Bromphenacylester. F. 152,6? (korr.) aus Alkohol oder Eisessig!?, 154,5? 13, 
Trennung von Korksáure. Adipinsáure ist in Äther schwerer, in Wasser 
leichter lóslich als Korksáure?. 
Bestimmung durch Titration in üblicher Weise. 
  
C,H,,0, M.G. 146 
C 49,3% 
H 6,9% 
  
  
  
  
177. Pimelinsäure. 
C,H,,0, = HOOC[CH;],COOH. 
Monoklin-prismatische Tafeln!5, PF. 105—106? (aus Wasser)", Kp.,49 272? 19. 
Unzersetzt sublimierbar!$. 
Naehweis. Dihydrazid?. F. 182? (aus Alkohol). Dipikrat #. 166°. 
p-Phenylphenacylester!*. F.145—148° (u. Zers.) aus 95proz. Alkohol. 
Phenacylester'?. F. 72,4° (aus Aceton). 
p-Bromphenacylester'3. F. 136,6? (aus Aceton). 
* ! RAMMELSBERG: À. Phys. 94, 519 (1855). 
B ? BOTTINGER: B. 11, 1352 (1878). 3 PERKIN: Soc. 53, 564 (1888). 
P 4 ROITHNER: M. 1%, 184 (1896). — MORRELL: Soc. 105, 2706 (1914). 
5 RATHER, REID: Am. soc. 41, 83 (1919). 
$ LADENBURG: A. 364, 230 (1909). 7 BRUGNATELLI: B. 29, 485 (1896). 
8 DieTERLE, HELL: B. 17, 2222 (1884). — Erris: Org. Synth. Sammelbd. I, 18 (1932). 
9 CIAMICIAN, SILBER: B. 29, 485 (1896). 
? Knarrr, NónpLINGER: B. 22, 818 (1889). 
1 Henry: C.r. 100, 944 (1885). 13 Curtis: J. pr. (2) 91, 4 (1915). 
13 KELLY, KLEFF: Am. soc. 54, 4444 (1932). 
14 DRAKE, SWEENEY: Am. soc. 54, 2060 (1932). 
15 LuND, LANGVAD: Am. soc. 54, 4107 (1932). 
16 v. Lana: M. 5, 359 (1884). — HAITINGER, LIEBEN: M. 5, 359 (1884). — DRUGMAN: 
Z. Kr. 53, 254 (1914). 
V AuwERS: À. 292, 151 (1896). 
fd 
18 VOLHARD: À. 26%, 81 (1892). 
  
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