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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 311. Vic. m-Xylenol.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

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die 
220 
ung 
ol4. 
33, 
144, 
er), 
1ge. 
ten 
04). 
17). 
— MI — 
311. Vie. m-Xylenol. 
CH, 
GHy0=< NOR. 
CH, 
Blättchen oder flache Nadeln!, 7. 49°23, Kp. 205° 3. 
Nachweis. Pikrat*. Orangegelbe Krystalle, F. 50—53°. 
p-Diphenylurethan®. .F. 198? (aus Alkohol, Benzol oder Benzol-Ligroin). 
1, 3-Dimethyl-2-phenoxyessigsäure®. F. 193,5° (aus Wasser). 
3, 5-Dinitrobenzoesäureester”, Tafeln, F. 158,8° (aus 95proz. Alkohol). 
Bestimmung nach ZEREWITINOFF: M. 371. 
312. Symm. m-Xylenol. 
HC 
CHO < OH. 
B,C 
Nadeln, P. 68? (aus Wasser)8, Ky. 219,5??. Sublimierbar$. 
Nachweis. p-Diphenylurethan?. F. 150° (aus Alkohol, Benzol oder Benzol- 
Ligroin). 
3, 0- Dinitrobenzoesdureester". Stübe, F. 195,4? (aus 95proz. Alkohol). 
1, 3-Dimethyl-5-phenoxyessigsäureS. F. 86° (aus Alkohol oder Benzol). 
Bestimmung nach ZEREWITINOFF: M. 371. 
313. m-Xylenol. 
CH, 
CH, = H,CC_ HOH. 
Nadeln, F. 25,4—26° 10, Ap. 211,5? (korr.)!3, Kp.,, 136°!12. Natriumsalz in 
Lauge leicht lôslich!?. 
Nachweis. p-Diphenylurethan5. F. 184° (aus Alkohol, Benzol oder Benzol- 
Ligroin). 
3, d-Dimitrobenzoat”. Tafeln, F. 164,6° (aus 95proz. Alkohol). 
1, 3-Dimethyl-6-phenoxyessigsäure%!3. Nädelchen, F, 141,6° (aus Benzol). 
Bestimmung nach ZEREWITINOFF: M. 371. 
314. p-Xylenol. 
CH, 
CH 0 = ( 0H : 
H.C 
Monoklin-prismatische 1* Krystalle, P. 74,5? (aus Alkohol) H, Kp..,, 211,5? 1!. 
Sublimierbar. Mit Wasserdampf flüchtig". 
Nachweis. Pikrat*. Orange Krystalle, P. 81—82°. 
p-Diphenylurethan?. P. 162? (aus Alkohol, Benzol oder Benzol-Ligroin). 
3, 0-Dinitrobenzoat". Nadeln, F. 137,2? (aus 95proz. Alkohol). 
| JACOBSEN: B. 12, 607 (1879). ? NöLTING: B. 21, 2829 (1888). 
3 GATTERMANN: A. 35%, 327 (1907). + BARIL, HAUBER: Am. soc. 53, 1087 (1931). 
$ MORGAN, PETTET: Soc. 1931, 1124. $ WERBA: Diss. Prag 1932. 
7 Puivurps, KEENAN: Am. soc. 53, 1924 (1931). 
$ NÖLTING, FOREL: B. 18, 2679 (1885). — ARMSTRONG, WILSON: Ch. News 83, 46 (1901). 
9 TöHL: B. 18, 362 (1885). 10 JACOBSEN: B. 18, 3464 (1885). 
11 JACOBSEN: B. 11, 24, 28 (1878). 12 AUWERS, CAMPENHAUSEN: B. 29, 1129 (1896). 
13 GLUUD, BREUER: Abh. K. Kohle 1917 II, 257. 14 JÄGER: Z. Kr. 38, 92 (1904). 
Meyer, Organische Verbindungen, 16

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