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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 385. Vanillin.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

     
   
  
  
   
   
  
  
   
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
  
   
    
     
    
    
  
     
OZ. 
204 
im- 
ck- 
gut 
ine, 
ich. 
oom 
oem. 
von 
iber 
ett, 
rot- 
orm 
der 
99). 
TER: 
30M: 
31). 
Wwe on 
ue eue 
. . 
— 297 — 
Bestimmung durch Titration mit Phenolphthalein als einbasische Säure: 
Hans MEYER: M. 24, 835 (1903). — THIEL, ROMER: Z. phys. 53, 742 (1908). — 
PAULY, SCHÜBEL, LOCKEMANN: A. 383, 311 (1911). In 20proz. Alkohol. 
Monoklin-prismatische! Nadeln, F.81—82° (aus Wasser oder Ligroin) 
  
C-H,0, M. G. 138 
6 60,9 96 
H 4,3% 
  
  
  
  
385. Vanillin. 
9 
C7 
Ni 
GHO- Hex »H 
HÓ 
2 
Träger des Geschmacks und Geruchs der Vanille®. Sublimierbar von 115° an?, 
Kp. 285° (im Kohlendioxydstrom)?, Kp.;5 170°¢. 
Naehweis. Über die mangelnde Verlüflichkeit der Farbreaktionen des Vanil- 
lins: Gildemeister, Hoffmann I, 537 (1928). 
5- Methylsemioxamazon?. F.2'0? (u. Zers.) aus Alkohol. 
Dimethon?. Kleine, prismatische Tafeln, F. 196—198° (korr.) aus Alkohol. 
Anhydrid Stäbchen, F.227— 228? (korr. aus Alkohol. 
Semicarbazon?. F.9232? (aus Eisessig durch Wasser). 
Thiosemicarbazon!?. Nadeln, F. 196—197? (aus Methylalkohol). 
p- 
Nitrobenzylüther*, F.194,5? (aus Alkohol durch Wasser). 
Phenallurethan??. PF. 116—117? (aus Alkohol). 
p- 
p- 
Bromphenylhydrazon' 1. P. 145,5? (aus Xylol). 
Naphthylhydrazon! 14, Schwach rosenrote, perlmutterglánzende Schuppen, 
F. 179° (aus Xylol). 
P- 
Nitrophenylhydrazon® 13. Rote Blättchen, F. 223° (aus Kisessig). 
m-Nitrobenzhydrazid!9. FF. 152°. 
Vanyllidendimethylbarbitursüure!$. Gelbe Blätter, F. 222,5—223° (aus Nitro- 
benzol. 
Bestimmung nach ZrrseL: M. 495. — Siehe dazu PHILLIPS: Analyst 48, 367 
(1923). 
Durch Titration!” mit Phenolphthalein. Auf 2% genau. 
1 
2 
3 
4 
5 
6 
7 
8 
SHADWELL: J. 1881, 602. 
Kemer: J. pr. (2) 78, 259 (1908). — Gildemeister, Hoffmann I, 536 (1928). 
TrEMANN: B. 4, 0614 (1874). 
NOELTING: A. ch. (8) 19, 481 (1910). 
TIEMANN, Korrr: B. 14, 2024 (1881). 
DRP. 63007 (1892). 
TIERIE: Rec. 52, 364 (1933). 
BERNARDI, TARTARINI: Ann. Chim. appl. 16, 132 (1926). — VORLANDER: Z. anal. 7%, 
241 (1929). 
9 
10 
11 
12 
13 
14 
15 
16 
17 
Orr: M. 26, 344 (1905). — PHILLIPS: Analyst 48, 367 (1923). 
FREUND, SCHANDER: B. 35, 2604 (1902). 
REID: Am. soc. 39, 307 (1917). 
Brapy, DUNN: Soc. 105, 2416 (1914). 
BILTZ, SIEDEN: A. 324, 319 (1902). — GRAZIANI: G. 43 II, 539 (1913). 
Hanus: Z. Nahr. 3, 531 (1900); 6, 817 (1903). 
HANUS: Z. Nahr. 10, 585 (1906). 
AKABORI: B. 66, 141 (1933). 
WELMANS: Pharm. Ztg. 1898, 634. — Hans Mryrr: M. 34, 837 (1903). — THIEL, 
ROMER: Z. phys. 63, 742 (1908). — Schimmel 1915, 55; 1923, 11. — RADCLIFFE, SHARPLES: 
Perf. Rec. 15, 396, 437 (1924). — Zanotti: Boll. ch. farm. 66, 33 (1927). — PFUND, JUNGE: 
B. 62, 515 (1929).

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