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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 16. Äthylnitrit.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

   
   
  
— 18 — 
Nachweis. Reaktion von Dovanury*!: Tief dunkelblaue Färbung. 
Bestimmung siehe unter Acetylentetrachlorid und $. 14. 
  
CHCl, M. G. 202 
  
  
  
C 11,9% 
H 0,5% 
CI 87,6%, 
  
13. Hexachloräthan. 
CCl, — CCI, + COL. 
Rhombisch-bipyramidale Tafeln (aus Alkohol-Ather), regulire Krystalle, die 
bei 71° triklin, bei 43,1° rhombisch werden (aus Anilin)?. F. 186,9—187,4° (korr.; 
im geschlossenen Róhrchen), Kp.,;;,185,5^?. Riecht campherartig. 
Nachweis. Beim Erhitzen mit alkoholischer Lauge auf 100? entstehen Athylen, 
Wasserstoff und Oxalsáure*. 
Reaktion von BEILSTEIN: M. 132. 
Bestimmung durch Hydrolyse 8. 14. 
  
GC, MG. 286,7 
C 10,1% 
Cl 89,9% 
  
  
  
  
14. Bromäthyl. 
C,H;Br — CH, - CH,Br. 
Farblose, àtherisch riechende Flüssigkeit, Kp.;,9 38,4 ^?. 
Prüfung. D.A.B. VI, 42 (1926). 
Nachweis. Reaktion von BEILSTEIN: M. 132. 
3-Nitrophthaläthylimid S. 17. 
Bestimmung S. 12. 
  
C,H,Br M. G. 109 
  
  
C 22,0% 
H 4,6% 
Br 13,4 96 
  
15. Jodäthyl. 
GELT CH, CH. 
Farblose Flüssigkeit, K.;4, 72,3? (korr.)$. 
Naehweis und Bestimmung S. 15. 
  
C,H M.G. 156 
  
  
  
C 15,4% 
H 3,2% 
J 81,4% 
  
16. Athylnitrit. 
C,H;0,N = CH, - CH, - O - NO. 
Angenehm obstartig riechende, süBlich und brennend schmeckende Flüssigkeit, 
Kp. 17°”. Mit Wasser mischbar. 
1 DovaHTy: Am. soc. 41, 1131 (1919). — S. 9. 
2 LEHMANN: Z. Kr. 6, 584 (1882). — ScHWARZ: Z. Kr. 25, 614 (1896). — STEINMETZ: 
Z. phys. 52, 466 (1905). — Pascan: C. r. 154, 886 (1912). 
3 STAEDEL: B. 11, 1738 (1878). 4 BERTHELOT: À. 109, 121 (1859). 
5 TYRER: Soc. 105, 2538 (1914). 
6 LINNEMANN: A. 160, 204 (1871). — CARRARA, CoPADORO: G. 331, 342 (1903). 
7 Mour: J. 1854, 561. — Brown: J. 1856, 575. 
  
  
   
  
  
   
    
    
  
  
  
  
  
  
   
   
   
   
   
   
     
  
  
  
   
   
  
  
   
   
    
  
  
   
  
   
   
     
  
  
  
  
  
  
   
  
     
Nagel 
Schwef 
schichte 
Best 
Schwefe 
gemisch 
+ HS 
sulfat t 
% Ath 
Nac 
Zu « 
lichen ? 
Chlorat. 
30 Minv 
n-Silber 
hg Rhe 
= 0,02: 
Formel: 
Nac] 
1 ce 
leem \ 
1 cem 2 
Durc 
Nach 
1: 7500 
Mit 
Quec 
1D. 
3 Hg 
4 Coc 
5 Nas 
6 Ru 
S TA 
3 KL.

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