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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 33. Sek. Isoamylalkohol.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

     
TASER PERRUNE 
=. 89 — 
Nachweis. Mit Piperonal! und 50 proz. Schwefelsäure Blaufärbung. 
Phenylurethan?. F.56,6° (aus Ligroin). 
p-Nitrophenylurethan®. F.97,5° (aus Tetrachlorkohlenstoff). 
x-Naphthylurethan*5. Dünne Tafeln, F.67—68° (aus verd. Alkohol). 
3, 5-Dinitrobenzoesäureester$. F.61—62° (aus Ligroin). «-Naphthylamin- 
verbindung F. 104—105° (aus Ligroin-Toluol). 
Anthrachinon-B-carbonsáureester. F.88—89° (aus Ligroin). 
Saurer 3-Nitrophthalsiureester?. F.165—166° (aus Wasser). 
Bestimmung nach ZzrsEL: M. 495. — Nach ZEREWITINOFF: M. 371 — 
B. 40, 2029 (1907). 
  
  
C,H,0 M.G.88 
6 68,2% 
H 13,6% 
  
  
  
  
32. Sek. Normalamylalkohol. 
(Hu « CH, - CH, - CH, - CH, (OH) - CH, . 
Flüssig, Kp.;,9 118,9?5. Lóslich in 6 Vol. Wasser?. 
Naehweis. Allophanat!'?. F.154? (aus Alkohol, Benzol oder Ligroin). 
x-Naphthylurethan®. Büschel feiner Nadeln, F.76—79° (aus Ligroin). 
3, 5-Dimitrobenzoesäureester!!. F.62,1° (aus 95proz. Alkohol). 
Bestimmung nach ZEISEL: M. 495. — Nach ZEREWITINOFF: M. 371. 
33. Sek. Isoamylalkohol. 
C,H,,0 — (CH;), - CH - CH(OH) - CH;. 
Flüssig, Kp.7ç9 111,3 —111,5° 812, 
Naehweis neben primárem Isoamylalkohol. Man löst in 3 T. 4,5 n-Brom- 
wasserstoff und erhitzt 1 Stunde im Einschlußrohr auf 100°. Der sekundäre 
Alkohol geht in Amylen über!?. 
Bestimmung nach Zersern: M. 495. — Nach ZerewiriNorr: M. 371. 
34. Tert. Butylearbinol. 
C.H,,0= (CH,)( - CH;OH. 
Pfefferminzähnlich riechende Krystalle, F. 52—53°18 14, Kp. 113°15, Sehr 
flüchtig. 
Nachweis. Phenylurethan!# 16. F. 114° (aus Ligroin). 
Semicarbazon des Brenztraubensäureesters!". F. 168°. 
Bestimmung nach ZEREWITINOFF: M. 371. 
! WEBER, Kocx: Ch. Ztg. 5%, 74 (1933). 
LEVINE, ALLEN: J. biol. chem. 27, 440 (1916). 
3 SHRINER, Cox: Am. soc. 53, 1604 (1931). 
4 FRENCH, BICKEL: Am. soc. 48, 747 (1926). 
5 NEUBERG, KANSKY: Bioch. 20, 445 (1909). 
6 
8 
t 
REICHSTEIN: Hel. 9, 802 (1926). 7 NICOLET, SACKS: Am. soc. 47, 2348 (1925). 
WILLCOx, BRUNEL: Am. soc. 38, 1838 (1916). Pickarp, KENYON: Soc. 99, 55 
(1911); 101, 627 (1912); 103, 1957 (1913). — d-Form 118,5—119,5°. 
9 BIELOHOUBEK: B. 9, 925 (1878). 
10 BéHar: Bull. (4) 25, 478 (1919). 11 MALONE, REID: Am. soc. 51, 3426 (1929). 
12 MICHAEL, ZEIDLER: À. 385, 262, 264 (1911). — d-Form F.110—112°: PICKARD, KENYON: 
Soc. 101, 630 (1912). 
13 'TTSSTER: A. ch. (6) 29, 340 (1893). 
14 WHITMORE, ROTHROCK: Am. soc. 54, 3431 (1932). 
15 SCHAUBLE, LôBL: M. 25, 1009 (1904). SAMEC: A. 351, 256 (1907). 
16 RICHARD: À. ch. (6) 21, 337 (1910). 17 BouvEAULT: C.r. 138, 984 (1904). 
  
  
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