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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 36. Tert. Amylalkohol, Amylenhydrat.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

      
    
  
  
  
  
   
   
   
  
  
  
   
    
    
  
  
   
   
      
     
  
  
  
  
  
  
    
    
     
  
   
    
  
ing. 
hol). 
hthylamin- 
M. 371 — 
roin). 
groin). 
‚371. 
4,5 n-Brom- 
° sekundäre 
„371. 
13°15, Sehr 
2348 (1925). 
: Soc. 99, 55 
, 9426 (1929). 
RD, KENYON: 
3, 984 (1904). 
REF EEE ESS APT RITES A N ET 
c 88 — 
Jo. Diäthylearbinol. 
C,H,,0 = CH, - CH, - CH(OH) - CH, - CH, 
Flüssig, Kp.7ç9 114,8—115,2°1. 
Nachweis. 3, 5-Dinitrobenzoesäureester?. Nadeln, F. 97° (aus 60 proz. Methyl- 
alkohol). 
Allophanat3. F.179,5° (aus Alkohol, Benzol oder Aceton). 
x-Naphthylurethan*. F.71—72° (aus Ligroin). 
Bestimmung nach ZEREWITINOFF: M. 371. 
36. Tert. Amylalkohol, Amylenhydrat. 
C,H,,0 — (CH,,C(OH) - CH, - CH,. 
Flüssig, P. —8,4?5, Kp.,,9 102,3?9 9. Lost sich in 8 T. Wasser. 
Prüfung. D.A.B. VI, 61 (1926). 
Nachweis. Die alkoholische Lösung gibt mit Schwefelsäure und 5proz. Wein- 
säure schön rosenrote Färbung” . 
Allophanat?. F.152° (aus Alkohol, Benzol oder Aceton). 
3, 5-Dinitrobenzoesäureester®. Monokline, längliche Platten®?, F. 117—118° 
(aus Ligroin). x-Naphthylaminderivat F. 123—129,5° (aus Ligroin-Toluol). 
Anthrachinon-B-carbonsäureester®. (Aus káuflichem Amylenhydrat.) F. 98 
bis 99° (aus Ligroin). 
x-Naphthylurethan"®. Lange, spieBige Tafeln, F.71—72° (aus Ligroin). 
Nachweis neben sek. Isoamylalkohol. Man erhitzt mit 7 T. 3n-Bromwasser- 
stoff 5 Minuten im EinschluBrohr auf 100°. Nur das Amylenhydrat geht in Tri- 
methylen über*!!. 
Bestimmung nach ZEREWITINOFF: M. 371 — B. 40, 2029 (1907). 
  
C,H,,0 M.G.88 
C 68,2% 
H 13,6% 
  
  
  
  
37. n-Hexylalkohol. 
C:Hy0 — CH,[CH, LCHLOH. 
Flüssig, Kp.7ç, 155,2°!12. Erstarrt in Kohlendioxyd-Ather 23, 
Nachweis. 3, d-Dinitrobenzoesäureester!*. F.60—61° (aus 95proz. Alkohol). 
x-Naphthylaminverbindung F. 103—104° (aus Ligroin-Toluol). 
Anthrachinon-f-carbonsäureester8. F. 88—89° (aus Ligroin). 
! WILLCOx, BRUNEL: Am. soc. 38, 1838 (1916). — PrCKARD, KENYON: Soc. 99, 55 (1911); 
101, 627 (1912); 103, 1957 (1913). — d-Form 118,5—119,5°. : 
BOEKSE, JONES, MAJOR: Am. soc. 53, 3530 (1931). 
BÉHAL: Bull. (4) 25, 478 (1919). 
BICKEL, FRENCH: Am. soc. 48, 749 (1926). 
TIMMERMANS: Bull. soc. ch. Belg. 3%, 334 (1914). 
ATKINS, WALLACE: Soc. 103, 1469 (1913). — JEFREMOW: Russ. 50, 361 (1920). 
EKKERT: Ph. Z. H. 66, 599 (1925). 5 RarcHsTEIN: Hel. 9, 802, 805 (1926). 
BRYANT: Am. soc. 54, 3762 (1932). 
NEUBERG, KANSKY: Bioch. 20, 445 (1909). 1! MICHAEL, ZEIDLER: A. 385, 262 (1911). 
12 WILLCOX, BRUNEL: Am. soc. 38, 1837 (1916). — MALONE, REID: Am. soc. 51, 3427 
(1929) 156,1°. — Kao, Ma: Se. rep. Tsing Hua Un. A 1, 181 (1932) 157°. 
13 FRENTZEL: B. 16, 744 (1883). 
14 REICHSTEIN: Hel. 9, 802 (1926). — MALONE, REID: Am. soc. 51, 3424 (1929). F. 58,4°. 
15 FRENCH, BICKEL: Am. soc. 48, 747 (1926). 
© 3 0 0 Sn OU m 
= 
e 
Meyer, Organische Verbindungen. 3

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