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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 38. n-Heptylalkohol.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

        
  
  
  
  
  
  
   
     
   
   
   
  
   
  
   
  
  
    
  
  
  
  
  
   
   
  
  
  
    
   
   
   
   
  
  
  
  
   
   
   
   
  
  
  
   
  
    
   
    
LS te 
it ire A re bi 
  
— 94 
p-Nitrophenylurethan!. F.103° (aus Tetrachlorkohlenstoff). 
p-Joddiphenylurethan?. Nadelfôrmige Prismen, F. 156, 1—156,3° (aus Tetra- 
chlorkohlenstoff). 
Allophanat?. F.165? (aus Alkohol, Benzol oder Aceton). 
Bestimmung nach ZEREWITINOFF: M. 371. 
Durch Oxydation mit Chromsäure: SEMICHON, FLANZY: C.r. 195, 254 (1932). 
  
C,H,,0 M.G. 102 
C 70,6 % 
H 13,7 % 
  
  
  
  
38. n-Heptylalkohol. 
C,H,,0 — CH, [CH CH,0H. 
Flüssig, F. —36,5°%, Kp.76, 172,5—173,5° 25, 
Nachweis. 3, 5-DinitrobenzoesäureesterS. F. 47—48,5^ (aus Ligroin). «-Naph- 
thylaminverbindung 57—58,5° (aus Ligroin-Toluol). 
Anthrachinon-B-carbonsäureester$. F.T6—77° (aus Ligroin). 
Phenylurethan”. F. 60° (aus Ligroin). 
x-Naphthylurethan8. Feine Nadeln, F. 62° (aus Ligroin). 
p-Nitrophenylurethan. F.102° (aus Tetrachlorkohlenstoff). 
p-Joddiphenylurethan?. F.150,1—150,9°. Nadeln (aus Tetrachlorkohlen- 
stoff), Platten (aus Aceton). 
Allophanat®. F.160° (aus Alkohol, Benzol oder Aceton). 
Bestimmung nach ZEREWITINOFF: M.371. 
Durch Oxydation mit Chromsáure: SEMICHON, FLANZY: C.r. 195, 254 (1932). 
  
O,H,,0 M.G. 116 
C 72,4% 
H. 155% 
  
  
  
  
39. n-Octylalkohol, Octanol-1. 
C,H,.0 == CH; : [CH;], » CH,OH. 
Flüssigkeit von durchdringendem Geruch, F. —15°°, Kp. 195,5° {korr. He U, 
196—197° 12, 
Nachweis. Phenylurethan'®. F.T4,2° (aus Ligroin). 
x-Naphthylurethan*. SpieBige Nadeln, F. 66° (aus Ligroin). 
p-Joddiphenylurethan?9. Nadeln, F. 148,2—149,2° (aus Tetrachlorkohlenstoff). 
1 SHRINER, Cox: Am. soc. 53, 1604 (1931). 
2 Kawar, TAMURA: Sc. pap. Inst. ph. ch. res. Tokyo 13, 270 (1930). — Kao, Ma: Sc. rep. 
Tsing Hua Un. A 1, 181 (1932) 176°. 
3 B£HAL: Bull. (4) 25, 477 (1919). 4 CARRARA, CoPPADORO: G. 331, 343 (1903). 
5 WILLCOX, BRUNEL: Am. soc. 38, 1837 (1916). — MALONE, REID: Am. soc. 51, 3427 
(1929) 156,1°. — Kao, Ma: Se. rep. Tsing Hua Un. A 1, 181 (1932) 157°. 
6 REICHSTEIN: Hel. 9, 802, 805 (1926). — Suoj1: Sc. pap. Inst. ph. ch. res. Tokyo 20, 
98 (1933). 
7 LEVINE, TAYLOR: J. biol. chem. 35, 283, 760 (1918). 
8 NEUBERG, KANSKY: Bioch. 20, 449 (1909). 
9 FRANCHIMONT: Rec. 16, 132 (1897). — CARRARA, CoPPADORO: G. 33 I, 343 (1903). 
F. —17,9°. — LEsriEAU: C.r. 158, 1188 (1914). F. — 14°, 
10 ZANDER: A. 224, 84 (1884). 
11 MALONE, REID: Am. soc. 51, 3426 (1929). — Kao, Ma: Sc. rep. Tsing Hua Un. A 1, 
181 (1932). 
12 Gildemeister, Hoffmann I, 419 (1928). 13 CHABLAY: À. ch. (9) 8, 215 (1917). 
14 NEUBERG, KANSKY: Bioch. 20, 445 (1909). 
15 KAwAI, TAMURA: Sc. pap. Inst. ph. ch. res. Tokyo 13, 270 (1930). 
EE EEE ETES ETES VERS PERS Iu Ud RE TT ST TETE RE ET 
p-Nù 
Benzol). 
Alloy 
3, 5-1 
Alkohol) 
Anth 
p-Nu 
Oxyd 
Besti 
Flüss 
Nach 
Alkohol) 
Anth 
Ligroin. 
Semi 
x-Na 
Allop 
Bestii 
Citroi 
213,57 1%: 
Naeln 
p-Jod 
chlorkoh 
Allop 
à, 9-1 
p-Nit 
  
1 VAN 
3 REr 
4 MAL 
181 (1932 
5 RE 
7 Gild 
9 Scm 
10 Sw 
11 KAB 
12 REI 
13 Bou 
14 FRE 
15 STE] 
16 Gild 
17 MAL 
18 KRA 
19 Kaw 
20 Hop

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