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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 52. Phytol.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

  
       
   
  
     
    
    
    
      
   
    
     
   
    
    
   
     
    
  
    
  
    
  
  
   
    
— A — 
  
  
  
  
  
  
Nr 12, 12 (1907). — SIMMONS: Analyst 40, 491 (1915). — Schimmel 1912 IT, 39; Bes 
1913 II, 60. — Prav: J. pr. (2) 102, 276 (1921). — BENNET: Perf. Rec. 12, 351 das Öl 
(1922). Na 
: à . à * 1,8 
Durch Acetylierung! 8.3. ^6 Citronellol = 2 00 — 0,64 
Nach ZEREWITINOFF2: M. 371. % Citronellol = 0,701 n Lósungsmittel in Gra 
Toluol (Xylol). 
C,H40 M. G. 156 
C 76,9% 
H 12,8% 
52. Phytol. . Na 
C,,H4,0 — CH,/CH V-- C-CH,0H. Kp.g5 | 
| ) Na« 
CHj/, CH; Verseil 
Farbloses Ol von schwachem Geruch.  Verursacht Kratzen im Halse. Di 
Kp.0,02—0,05 145°>. lich in 
Nachweis. Natriumsalz?. Leicht löslich in Äther und Petroläther. Tet 
Phenylurethan®. F.25,8—28,8° (aus Hexan, dann Methylalkohol). Essige: 
x-Naphthylurethan?. Radial angeordnete Nadeln, P. 23,5—29,5^ (aus Methyl- Bes 
alkohol). lumen 
Phthalestersiure®. Sirup. Silbersalz (aus Benzol + Methylalkohol). Mikro- Cramn 
skopisch kleine, flache Prismen, F. 119? (x-Phytol), 116? (6-Phytol; Prismen aus Du 
Alkohol). In Äther, Benzol und heißem Alkohol leicht, in Methylalkohol schwer 319 (1 
löslich. 
Bestimmung. Addiert in Chloroform 1 Mol. Brom (bei 0^) ?. 
Siehe auch WILLSTÄTTER, STOLL: Chlorophyll 1913, 309. 
C,H4,0 M. G. 296 
C 81,1% 
H 13,5% 
  
  
  
  
  
  
  
Ro: 
. Na 
53. Linalool. Di 
$- 
CH, LI 
H,C | Di 
C,,H,,0 — E oh :OH—COH,-CH,-O- GH: CH,. 1500— 
: | 
: OH B-A 
Maiglöckchenähnlich riechendes Öl, Kp. 199—9200?5. 4,5» 0,8666. Reinigung t s 
über das Natriumsalz des Phthalsáureesters?, das durch alkoholisches Kali ver- ramon 
seift wird und Atherextraktion (nicht Destillation mit Wasserdampf!) oder durch 1 
Spaltung des Phenylurethans?. Gibt kein krystallinisches Allophanat*. DS 
Nachweis. Phenylurethan®. Nadeln, F. 65—066*? (aus verd. Alkohol). Die in- Roure-1 
aktive Form hat F'.63—65^?. Nr 
«-Naphthylurethan'®. F.53°1 (aus verd. Methylalkohol). 18, 158 
À 3 7 
1 Schimmel 1894 II, 65. ? ZEREWITINOFF: Z. anal. 68, 325 (1926). 5 B 
3 WILLSTATTER, HOCHEDER: À. 354, 245 (1907). 7B 
4 WILLSTATTER, HÜNI: A. 378, 84 (1911). 8G 
5 Schimmel 1911 II, 139. 9 T 
6 TIEMANN: B. 31, 837 (1898). — CHARABOT: À. ch. (7) 21, 232 (1900). FLATTA 
7 BéHaL: Bull. (4) 25, 452 (1919). 108 
8 WALBAUM, HÜürH1G: J. pr. (2) 6%, 823 (1903). 1 B 
9 RUzICKA, FORNASIR: Hel. 3, 186 (1919). 12 K 
19 Schimmel 1906 II, 32. 11 Gildemeister, Hoffmann I, 428 (1928). 13 FF 
SALARIES 
fe ET RTE EP TT RE RETRO EE EEE TR ERET

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Meyer, Hans. Nachweis Und Bestimmung Organischer Verbindungen. Verlag von Julius Springer, 1933.

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