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Nachweis und Bestimmung organischer Verbindungen (2. Band)

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fullscreen: Nachweis und Bestimmung organischer Verbindungen (2. Band)

Multivolume work

Persistent identifier:: 1670259072

Author:: Meyer, Hans

Title:: Lehrbuch der organisch-chemischen Methodik

Type of content:: Lehrbuch

Year of publication:: 1922

Place of publication:: Wien

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670259072

Language:: German

Additional Notes:: Bände 1-3,2 erschienen von 1922-1940

Document type:: Multivolume work

Volume

Persistent identifier:: 1670273296

Author:: Meyer, Hans

Title:: Nachweis und Bestimmung organischer Verbindungen

Sub title:: mit 11 Abbildungen

Scope:: XII, 426 Seiten

Type of content:: Lehrbuch

DOI:: 10.14463/KXP:1670273296

Year of publication:: 1933

Place of publication:: Berlin

Publisher of the original:: Verlag von Julius Springer

Identifier (digital):: 1670273296

Illustration:: Illustrationen

Signature of the source:: a 368(2)

Language:: German

Usage licence:: Public Domain Mark 1.0

Publisher of the digital copy:: Technische Informationsbibliothek Hannover

Place of publication of the digital copy:: Hannover

Year of publication of the original:: 2019

Document type:: Volume

Collection:: Chemistry

Chapter

Title:: 54. Nerol.

Document type:: Multivolume work

Structure type:: Chapter

Contents

Table of contents

Full text

      
    
   
  
  
  
    
    
  
  
     
    
   
   
    
    
   
   
  
   
  
    
     
   
   
   
    
    
    
   
  
    
   
    
1912 II, 39; 
vec. 12, 351 
sungsmittel 
im Halse. 
er. 
1). 
aus Methyl- 
ol). Mikro- 
Prismen aus 
ohol schwer 
Reinigung 
's Kali ver- 
oder durch 
at". 
ol). Die in- 
73 
EE AT a A SA EA GA AE NE RSEE TS EEE 
eoi —. nettes” AI UNE e sr * = 
— 41 —— 
Bestimmung gelingt halbwegs durch Ermittlung der Acetylzahl^?, wobei 
das Öl mit Terpentinöl, Xylol od. dgl. verdünnt werden muß. M. 331. — S.3. 
Nach ZEREWITINOFF3: M. 371. Lôsungsmittel Toluol oder Xylol. % Linalool 
= 0,692 E . V — Anzahl eem Methan (0?, 760 mm), S — Gewicht der Substanz 
in Grammen. 
54. Nerol. 
H,C 
e SC:CH-CH,-CH,-C- CH,. 
HO - CH, - CH 
Namentlich in der Verdiinnung roseniahnlich riechendes Ol, K.,,, 226— 227^, 
Kp.,5 125^ 1. 
Naehweis. Allophanat?. PF. 101,5? (aus Alkohol). Zur Reinigung geeignet. 
Verseifbar durch kochende verdünnte Lauge. 
Diphenylurethan$. F. 52—53° (aus Methylalkohol oder Pentan). Bei 0? lós- 
lich in 13—14 T. Pentan, 120 T. Methylalkohol (Trennung von Geraniol!). 
Tetrabromid$. Lange, seidenglánzende Nadeln, F.118—119° (aus wenig 
Essigester + viel Petrolédther). y 
Bestimmung nach ZzEgREWITINOFF?: M. 371. % Nerol = 0,672 = V — Vo- 
C,,H4,0 = 
lumen des ausgeschiedenen Methans (0?, 760 mm), S — Gewicht der Probe in 
Grammen. Lösungsmittel Toluol oder Xylol. 
Durch Titration mit Brom: MOoORRELL, LEVINE: Ind. eng. ch. An. ed. 4, 
319 (1932). 
55. Geraniol. 
NH 
H -C-CHOH 
Rosenartig riechendes Ol, Kp.757 220—230°78, Kp.,, 114—115° 89, 
Nachweis. Tetrabromid®. F.70—71°. «-Napthylurethan®. F. 47—48°. 
Di-f-Naphthylurethan". F.105—107°. 
Diphenylurethant. F. 82° (aus Ligroin). Bei 0° in 100—110 T. Pentan, 
1500—2000 T. Methylalkohol löslich. 
p-Anthrachinonylurethan®. Orangerote Krystalle, F. 173° (aus Xylol). 
Phihalestersäure. F.47°. Silbersalz F. 133°. Dient zu Bestimmungen (Ti- 
tration) #13, Tetrabromid!!. F. 114—115°. 
  
! Gildemeister, Hoffmann I, 428 (1928). 
? SIMMONS: Chemist-Druggist 70, 496 (1907). — BouLEz: Bull. (4) 1, 117 (1907). — 
Roure-Bertrand fils (2) 6, 73 (1907); 7, 35 (1908). — Schimmel 1907 I, 121, 128; 1909 II, 32; 
1910 L, 103; 1910 IL 154. — WarnBAUM, MULLER: Wallach-F. 654 (1909). — JEANCARD, 
SATIE: Am. Druggist 56, 42 (1910). — FERNANDEZ, LUENGO: A. soc. espafi. fis. quim. (2) 
18, 158 (1921). — Siehe S. 3. 
3 ZEREWITINOFF: Z. anal. 68, 321 (1926). * Gildemeister, Hoffmann I, 436 (1928). 
5 BÉHAL: Bull. (4) 25, 452 (1919). $ SopEN, TrErr: B. 39, 908 (1906). 
?* BERTRAM, GILDEMEISTER: J. pr. (2) 56, 508 (1899). 
5 Gildemeister, Hoffmann I, 430 (1928). 
? TIEMANN, SEMMLER: B. 36, 2711 (1893). — ERDMANN: J. pr. (2) 56, 3 (1897). — 
Frarrav, LABBÉ: C.r. 126, 1725 (1898). — STEPHAN: J. pr. (2) 60, 248 (1899). 
10 Schimmel 1906 II, 38. — Gildemeister, Hoffmann I, 434 (1928). 
!1 BLUMANN, ZEITSCHEL: B. 44, 2593 (1911). — PıLLEY: Soc. Ind. 47, 52 (1928). 
1? Kawar, TAMURA: Sc. pap. Inst. ph. ch. res. Tokyo 13, 1970 (1930). 
13 FrATTAU, LABBÉ: C. r. 126, 1725 (1898).

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