Prakt. Met. Sonderband 38 (2006) 165
phases can be clearly distinguished. In Fig. 2b the dendritic y, phase prevails. Two
sample different grey-tones suggest two different crystallographic orientations. One for v2 on the
samples grain boundaries (darker grey) and one for intragranular y, (lighter grey). In the inter-
dendritic space the characteristic martensitic pattern can be observed, consisting of
es (lISE differently oriented plates. The thin bright horizontal lines observable in Fig. 2b could be
electron one of the FIB artefacts: The ion-current 10 pA was rather low (and consequently the
diameter of the beam small) for FIB-etching the area of about 450 um“, Therefore, it could
have happened that the surface was unevenly “covered” by the beam.
with six
n alloy 1
ng times
ng time.
> to their
t parallel
ss have
ions the
veloped
inning of
‚1a and
polished
must be
g of the Figure 2: Cross-section of an alloy 2 (Cu — 15 wt% Al — 4 wt% Ni) melt-spun ribbon;
a) Mechanically polished; b) The same area after 1 hour FIB-etching with 10 pA.
1anically
1. Figure 3: The wheel-side surface of an alloy 2 melt-spun ribbon; a) In as-cast condition; b)
After 90 minutes of FIB-etching, using ion current of 10 pA
nd after
3 ribbon