Full text: Fortschritte in der Metallographie

338 Prakt. Met. Sonderband 52 (2018) 
5. SUMMARY AND OUTLOOK 
* A dense steel matrix composite with 10 vol.% TiC was produced by powder blending, 
HIP consolidation and heat treatment. 
The formation of a reaction phase between TiC and the steel matrix was confirmed by 
SEM and XRD, whereas its chemical composition was found to be (Ti,M)C with M = V, 
Mo, W, Cr, Fe) by STEM/EDS. 
It was established by quantitative analysis of SEM/BSE images and XRD, that with 
increasing HIP time the reaction phase increases, although reaction kinetics slow down 
towards higher HIP times. 
In future works Rietveld refinement will be applied and the different scattering factors of 
TiC and (Ti,M)C will be taken into account to study reaction phase fraction and formation 
kinetics in detail. 
REFERENCES 
[1] K. I. Parashivamurthy, R. K. Kumar, S. Seetharamu and M. N. Chdrasekharaiah: 
"Review on TiC reinforced steel composites”, J. Mater. Sci. no. 36, pp. 4519-4530, 2001. 
[2] K. Das, S. Bandyopadhyay and S. Das: "A Review on the various synthesis routes of 
TiC reinforced ferrous based composites", J. Mater. Sci., vol. 37, pp. 3881-3892, 2002. 
[3] C. Jin and K. P. Plucknett: "Microstructure instability in TiC-316L stainless steel 
cermets”, Int. J. Refract. Met. Hard Mater., vol. 58, pp. 74-83, 2016. 
[4] H. Hill, S. Weber, S. Huth, P. Niederhofer and W. Theisen: "The impact of processing 
on microstructure, single-phase properties and wear resistance of MMCs", Wear, vol. 271, 
pp. 1895-1902, 2011. 
[5] E. Pagounis, M. Talvitie and V. K. Lindroos: "Microstructure and Mechanical 
Properties of Hot Work Tool Steel Matrix Composites Produced by Hot Isostatic Pressing", 
Powder Metall., vol. 40, no. 1, pp. 55-61, 1997. 
[6] J. Pérnbacher, S. Marsoner, H. Leitner and G. Ressel: "Interaction of Particulate TiC 
in a Steel-Based MMC: A Thermodynamic Approach on Phase Compositions," Euro 
PM2018 Proceeding, To be published. 
[7] D. Cédat, C. Rey, M. Clavel, J. Schmitt, M. Le Flem and A. Allemand: "Microstructural 
characterization of a composite Mo reinforced by 25 at.% TiC", J. Nucl. Mater. vol. 385, pp. 
533-537, 2009. 
[8] R. Wirth: "Focused lon Beam (FIB) combined with SEM and TEM: Advanced 
analytical tools for studies of chemical composition, microstructure and crystal structure in 
geomaterials on a nanometre scale" Chem. Geol., vol. 261, pp. 217-229, 2009. 
[9] J.-M. Song, Y.-J. Wang, Y. Zhou: "Thermomechanical properties of TiC particle- 
reinforced tungsten composite for high temperature applications”, Int. J. Refract Met. H., vol. 
21, pp. 1-12, 2003 
[10] M. Oliveira, J. Bolton: “Sintering of M3/2 High Speed Steel Modified by Additions of 
Copper Phosphide and Titanium Based Ceramic Compounds." Powder Metallurgy, vol. 38, 
no. 2, pp. 131-140, 1995 
[11] J. H. Jang, C.-H. Lee, Y.-U. Heo, D.-W. Suh: "Stability of (Ti,M)C (M = Nb, V, Mo, and 
W) carbide in steels using first-principles calculations", Acta Mater., vol. 60, pp. 208-217, 
2012. 
[12] P.A. Silva, S. Weber, G. inden, A.R. Pyzalla: “Influence of hard particle addition and 
chemical interdiffusion on the properties of hot extruded tool steel compounds”, Mater. Sci. 
Eng. A, vol. 516, 2009
	        
Waiting...

Note to user

Dear user,

In response to current developments in the web technology used by the Goobi viewer, the software no longer supports your browser.

Please use one of the following browsers to display this page correctly.

Thank you.